From bbc070b45ad6ba43bf7ed34e47a49ef9a727f806 Mon Sep 17 00:00:00 2001 From: TaoS Date: Thu, 25 Jul 2024 02:01:30 +0800 Subject: [PATCH] =?UTF-8?q?=E4=B8=8A=E4=BC=A0=E6=96=87=E4=BB=B6=E8=87=B3?= =?UTF-8?q?=20/?= MIME-Version: 1.0 Content-Type: text/plain; charset=UTF-8 Content-Transfer-Encoding: 8bit --- Characterizing_azobenzene_molecules.xml | 12 ++++++++++++ ...esizing_bismuth_oxyhalides_and_testing.xml | 19 +++++++++++++++++++ ...graphitic_carbon_nitrides_and _testing.xml | 14 ++++++++++++++ ...atalysts_for_oxygen_evolution_reaction.xml | 19 +++++++++++++++++++ ...sizing_metal_oxides_and_characterizing.xml | 17 +++++++++++++++++ 5 files changed, 81 insertions(+) create mode 100644 Characterizing_azobenzene_molecules.xml create mode 100644 Synthesizing_bismuth_oxyhalides_and_testing.xml create mode 100644 Synthesizing_graphitic_carbon_nitrides_and _testing.xml create mode 100644 Synthesizing_metal-organic_high-entropy_catalysts_for_oxygen_evolution_reaction.xml create mode 100644 Synthesizing_metal_oxides_and_characterizing.xml diff --git a/Characterizing_azobenzene_molecules.xml b/Characterizing_azobenzene_molecules.xml new file mode 100644 index 0000000..d4492ea --- /dev/null +++ b/Characterizing_azobenzene_molecules.xml @@ -0,0 +1,12 @@ + + Characterizing azobenzene molecules by infrared spectroscopy + + Retrieve the rack from the sample rack station. + Use the solid station to add 0.18 g of azobenzene. + Use the liquid station to add 8 g of dichloromethane. + Use the magnetic stirring station to stir the mixture at 500 rpm for 10 minutes at 25 ℃. + Use the sample preparation station to make the sample of azobenzene. + Use the infrared spectroscopy station to test the infrared spectrum of the sample. + Place the rack into the sample rack station. + + diff --git a/Synthesizing_bismuth_oxyhalides_and_testing.xml b/Synthesizing_bismuth_oxyhalides_and_testing.xml new file mode 100644 index 0000000..8a613d2 --- /dev/null +++ b/Synthesizing_bismuth_oxyhalides_and_testing.xml @@ -0,0 +1,19 @@ + + Synthesizing bismuth oxyhalides and measuring photocatalytic degradation of tetracycline by UV-vis spectroscopy + + Retrieve the rack from the sample rack station. + Use the solid station to add 0.195 g of Bi(NO3)3•5H2O. + Use the liquid station to add 10 g of deionized water. + Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃. + Use the solid station to add 0.035 g NaCl. + Use the magnetic stirring station to stir the mixture at 600 rpm for 1 hour at 25 ℃. + Use the drying station to dry the sample at 60 ℃ for 6 hours. + Use the solid station to add 0.005 g of BiOCl. + Use the liquid station to add 10 g of tetracycline aqueous solution. + Use the magnetic stirring station to stir the mixture at 600 rpm for 30 minutes at 25 ℃. + Use the photocatalytic station to perform photocatalytic test for 30 minutes. + Use the centrifuge station to centrifuge at 5000 rpm for 10 minutes. + Use the UV-vis spectroscopy station to test the sample. + Place the rack into the sample rack station. + + diff --git a/Synthesizing_graphitic_carbon_nitrides_and _testing.xml b/Synthesizing_graphitic_carbon_nitrides_and _testing.xml new file mode 100644 index 0000000..672246c --- /dev/null +++ b/Synthesizing_graphitic_carbon_nitrides_and _testing.xml @@ -0,0 +1,14 @@ + + Synthesizing graphitic carbon nitrides and measuring photocatalytic hydrogen production by gas chromatography + + Retrieve the rack from the sample rack station. + Use the solid station to add 5 g of dicyandiamide. + Use the calcination station to heat the sample to 500 ℃ for 3 hours with a heating rate of 2 ℃/min. + Use the liquid station to add 1 g of triethanolamine. + Use the liquid station to add 9 g of H2PtCl6 solution. + Use the encapsulation station to encapsulate the reaction vessel under vacuum. + Use the photocatalytic station to perform photocatalytic test for 1 hour. + Use the gas chromatography station to detect the produced gas. + Place the rack into the sample rack station. + + diff --git a/Synthesizing_metal-organic_high-entropy_catalysts_for_oxygen_evolution_reaction.xml b/Synthesizing_metal-organic_high-entropy_catalysts_for_oxygen_evolution_reaction.xml new file mode 100644 index 0000000..f7283ef --- /dev/null +++ b/Synthesizing_metal-organic_high-entropy_catalysts_for_oxygen_evolution_reaction.xml @@ -0,0 +1,19 @@ + + Synthesizing metal-organic high-entropy catalysts for oxygen evolution reaction + + Retrieve the rack from the sample rack station. + Use the liquid station to add 2 g of cobalt acetate solution. + Use the liquid station to add 2 g of nickel acetate solution. + Use the liquid station to add 2 g of iron acetate solution. + Use the liquid station to add 2 g of manganese acetate solution. + Use the liquid station to add 2 g of copper acetate solution. + Use the liquid station to add 5 g phthalic acid solution. + Use the magnetic stirring station to stir the mixture at 500 rpm for 24 hours at 25 ℃. + Use the centrifuge station to centrifuge at 5000 rpm for 3 minutes. + Use the aspiration station to aspirate the liquid above the sample after centrifugation. + Use the liquid station to add 8 g Nafion solution. + Use the sample preparation station to make the sample of MO-HEC. + Use the electrocatalytic station to perform electrochemical tests. + Place the rack into the sample rack station. + + diff --git a/Synthesizing_metal_oxides_and_characterizing.xml b/Synthesizing_metal_oxides_and_characterizing.xml new file mode 100644 index 0000000..c04259f --- /dev/null +++ b/Synthesizing_metal_oxides_and_characterizing.xml @@ -0,0 +1,17 @@ + + Synthesizing metal oxides and characterizing by PXRD + + Retrieve the rack from the sample rack station. + Use the solid station to add 0.2 g of ZrCl4. + Use the liquid station to add 10 g of ethanol. + Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃. + Use the solid station to add 0.03 g graphene. + Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃. + Use the drying station to dry the sample at 80 ℃ for 2 hours. + Use the calcination station to heat the sample to 400 ℃ for 6 hours with a heating rate of 5 ℃/min. + Use the liquid station to add 5 g of ethanol. + Use the sample preparation station to make the sample of metal oxide. + Use the PXRD station to characterize the PXRD pattern of the sample. + Place the rack into the sample rack station. + +