Jiang_Group.USTC/warehouse_for_experimental_protocols
2
0
Fork 0
Code Issues Pull Requests Packages Projects Releases Wiki Activity

上传文件至 /

Browse Source
This commit is contained in:
TaoS 2024-07-25 02:01:30 +08:00
parent 04348e5dd7
commit bbc070b45a
5 changed files with 81 additions and 0 deletions
Show Stats Download Patch File Download Diff File Expand all files Collapse all files

12
Characterizing_azobenzene_molecules.xml Normal file
View File

@ -0,0 +1,12 @@
<experiment id="exp001">
<Type>Characterizing azobenzene molecules by infrared spectroscopy</Type>
<Procedure>
<Step number="1">Retrieve the rack from the sample rack station.</Step>
<Step number="2">Use the solid station to add 0.18 g of azobenzene.</Step>
<Step number="3">Use the liquid station to add 8 g of dichloromethane.</Step>
<Step number="4">Use the magnetic stirring station to stir the mixture at 500 rpm for 10 minutes at 25 ℃.</Step>
<Step number="5">Use the sample preparation station to make the sample of azobenzene.</Step>
<Step number="6">Use the infrared spectroscopy station to test the infrared spectrum of the sample.</Step>
<Step number="7">Place the rack into the sample rack station.</Step>
</Procedure>
</experiment>

19
Synthesizing_bismuth_oxyhalides_and_testing.xml Normal file
View File

@ -0,0 +1,19 @@
<experiment id="exp001">
<Type>Synthesizing bismuth oxyhalides and measuring photocatalytic degradation of tetracycline by UV-vis spectroscopy</Type>
<Procedure>
<Step number="1">Retrieve the rack from the sample rack station.</Step>
<Step number="2">Use the solid station to add 0.195 g of Bi(NO3)3•5H2O.</Step>
<Step number="3">Use the liquid station to add 10 g of deionized water.</Step>
<Step number="4">Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃.</Step>
<Step number="5">Use the solid station to add 0.035 g NaCl.</Step>
<Step number="6">Use the magnetic stirring station to stir the mixture at 600 rpm for 1 hour at 25 ℃.</Step>
<Step number="7">Use the drying station to dry the sample at 60 ℃ for 6 hours.</Step>
<Step number="8">Use the solid station to add 0.005 g of BiOCl.</Step>
<Step number="9">Use the liquid station to add 10 g of tetracycline aqueous solution.</Step>
<Step number="10">Use the magnetic stirring station to stir the mixture at 600 rpm for 30 minutes at 25 ℃.</Step>
<Step number="11">Use the photocatalytic station to perform photocatalytic test for 30 minutes.</Step>
<Step number="12">Use the centrifuge station to centrifuge at 5000 rpm for 10 minutes.</Step>
<Step number="13">Use the UV-vis spectroscopy station to test the sample.</Step>
<Step number="14">Place the rack into the sample rack station.</Step>
</Procedure>
</experiment>

14
Synthesizing_graphitic_carbon_nitrides_and _testing.xml Normal file
View File

@ -0,0 +1,14 @@
<experiment id="exp005">
<Type>Synthesizing graphitic carbon nitrides and measuring photocatalytic hydrogen production by gas chromatography</Type>
<Procedure>
<Step number="1">Retrieve the rack from the sample rack station.</Step>
<Step number="2">Use the solid station to add 5 g of dicyandiamide.</Step>
<Step number="3">Use the calcination station to heat the sample to 500 ℃ for 3 hours with a heating rate of 2 ℃/min.</Step>
<Step number="4">Use the liquid station to add 1 g of triethanolamine.</Step>
<Step number="5">Use the liquid station to add 9 g of H2PtCl6 solution.</Step>
<Step number="6">Use the encapsulation station to encapsulate the reaction vessel under vacuum.</Step>
<Step number="7">Use the photocatalytic station to perform photocatalytic test for 1 hour.</Step>
<Step number="8">Use the gas chromatography station to detect the produced gas.</Step>
<Step number="9">Place the rack into the sample rack station.</Step>
</Procedure>
</experiment>

19
Synthesizing_metal-organic_high-entropy_catalysts_for_oxygen_evolution_reaction.xml Normal file
View File

@ -0,0 +1,19 @@
<experiment id="exp001">
<Type>Synthesizing metal-organic high-entropy catalysts for oxygen evolution reaction</Type>
<Procedure>
<Step number="1">Retrieve the rack from the sample rack station.</Step>
<Step number="2">Use the liquid station to add 2 g of cobalt acetate solution.</Step>
<Step number="3">Use the liquid station to add 2 g of nickel acetate solution.</Step>
<Step number="4">Use the liquid station to add 2 g of iron acetate solution.</Step>
<Step number="5">Use the liquid station to add 2 g of manganese acetate solution.</Step>
<Step number="6">Use the liquid station to add 2 g of copper acetate solution.</Step>
<Step number="7">Use the liquid station to add 5 g phthalic acid solution.</Step>
<Step number="8">Use the magnetic stirring station to stir the mixture at 500 rpm for 24 hours at 25 ℃.</Step>
<Step number="9">Use the centrifuge station to centrifuge at 5000 rpm for 3 minutes.</Step>
<Step number="10">Use the aspiration station to aspirate the liquid above the sample after centrifugation.</Step>
<Step number="11">Use the liquid station to add 8 g Nafion solution.</Step>
<Step number="12">Use the sample preparation station to make the sample of MO-HEC.</Step>
<Step number="13">Use the electrocatalytic station to perform electrochemical tests.</Step>
<Step number="14">Place the rack into the sample rack station.</Step>
</Procedure>
</experiment>

17
Synthesizing_metal_oxides_and_characterizing.xml Normal file
View File

@ -0,0 +1,17 @@
<experiment id="exp001">
<Type>Synthesizing metal oxides and characterizing by PXRD</Type>
<Procedure>
<Step number="1">Retrieve the rack from the sample rack station.</Step>
<Step number="2">Use the solid station to add 0.2 g of ZrCl4.</Step>
<Step number="3">Use the liquid station to add 10 g of ethanol.</Step>
<Step number="4">Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃.</Step>
<Step number="5">Use the solid station to add 0.03 g graphene.</Step>
<Step number="6">Use the magnetic stirring station to stir the mixture at 600 rpm for 10 minutes at 25 ℃.</Step>
<Step number="7">Use the drying station to dry the sample at 80 ℃ for 2 hours.</Step>
<Step number="8">Use the calcination station to heat the sample to 400 ℃ for 6 hours with a heating rate of 5 ℃/min.</Step>
<Step number="9">Use the liquid station to add 5 g of ethanol.</Step>
<Step number="10">Use the sample preparation station to make the sample of metal oxide.</Step>
<Step number="11">Use the PXRD station to characterize the PXRD pattern of the sample.</Step>
<Step number="12">Place the rack into the sample rack station.</Step>
</Procedure>
</experiment>